Desenvolvimento e validação do método QuEChERS na determinação de resíduos de medicamentos veterinários em leite e carne de búfalo.
| dc.contributor | SILVIA H. G. BRONDI; GILBERTO BATISTA DE SOUZA, CPPSE; ANA RITA DE ARAUJO NOGUEIRA, CPPSE; LAÍS A. DE CAMARGO, Universidade Federal de São Carlos; RAFAELA F. MAJARON, Universidade Federal de São Carlos. | |
| dc.creator | BRONDI, S. H. G. | |
| dc.creator | SOUZA, G. B. de | |
| dc.creator | NOGUEIRA, A. R. de A. | |
| dc.creator | CAMARGO, L. A. DE | |
| dc.creator | MAJARON, R. F. | |
| dc.date | 2023-05-15T10:47:45Z | |
| dc.date | 2023-05-15T10:47:45Z | |
| dc.date | 2013-06-27 | |
| dc.date | 2013 | |
| dc.date.accessioned | 2026-07-07T05:31:49Z | |
| dc.description | Analytical methods were developed and validated to determine residues of veterinary drugs in buffalo milk and meat, using the QuEChERS method and gas chromatography-mass spectrometry. Both milk and meat, at 2 g of sample, 4 mL of acetonitrile, 0.8 g of MgSO4 and 0.2 g of NaCl, were used in the liquid-liquid partition, whereas 50 mg of C18, 50 mg of PSA and 150 mg of MgSO4 were employed in the dispersive solid-phase extraction (d-SPE). The methods showed sensitivity, precision and accuracy. The quantitation limits were in agreement with the maximum residue limit established by the Codex Alimentarius, FAO and WHO. | |
| dc.identifier | Química Nova, v. 36, n. 1, p. 153-158, 2013. | |
| dc.identifier | http://www.alice.cnptia.embrapa.br/alice/handle/doc/960760 | |
| dc.identifier | https://doi.org/10.1590/S0100-40422013000100025 | |
| dc.identifier.uri | http://hdl.handle.net/123456789/493954 | |
| dc.language | por | |
| dc.rights | openAccess | |
| dc.subject | CG EM | |
| dc.subject | QuEChERS method | |
| dc.subject | Veterinary drug | |
| dc.title | Desenvolvimento e validação do método QuEChERS na determinação de resíduos de medicamentos veterinários em leite e carne de búfalo. | |
| dc.type | Artigo de periódico |
